Parr-instrument Series 5500 Manual do Utilizador descarregar pdf (Página 2)

Compact Mini Bench Top Reactors

Parr Instrument Company

2

PREFACE 3

Scope 3

Related Instructions 3

Intended Usage 3

Safety Information 3

General Speciﬁcations 3

Explanation of Symbols 4

Environmental Conditions 4

Unpack Carefully 4

Provisions for Lifting and Carrying 4

Cleaning & Maintenance 4

User’s Responsibility 5

INSTALLATION 6

Flat PTFE Gasket 6

Self Sealing O-Ring Closure 6

Pressure and Temperature Limits 7

Assemble The Reactor 8

Motor Coupling Connection/Operation 8

IDENTIFY THE VALVES 10

Gas Inlet Valve 10

Gas Release Valve 10

Liquid Sampling Valve 10

OTHER VESSEL HEAD FITTINGS 11

Safety Rupture Disc 11

Type J Thermocouple 11

Pressure Gage 11

ACCESSORIES 11

Liners 11

Spare Parts Kit 11

HOW TO USE THE VESSEL 12

To open the Vessel 12

Before Closing the Vessel 12

Sealing Vessels with PTFE Gaskets 12

Sealing with Flexible Graphite Gaskets 12

O-ring Closures 12

Gas Connections 12

Pressurizing the Vessel 12

Do Not Overﬁll the Vessel 13

Releasing Pressure 13

Withdrawing Liquid Samples 13

Initial Operating Test 13

Internal Cooling Loop 13

MAINTENANCE 14

General Maintenance Notes 14

Periodic Pressure Tests 14

Technical Support 15

PARTS LISTS 16

Reaction Vessel Parts List 17

Vessel Heaters Parts List 19

DRAWINGS 20

Motor/Overarm Layout 20

Tach Option Layout 20

100, 160, 300 mL Mini Compact Reactor 21

450 mL Mini Compact Reactor 22

600 mL Mini Compact Reactor 23

Customer Service

Questions concerning the installation or operation

of this instrument can be answered by the Parr

Customer Service Department:

1-309-762-7716 • 1-800-872-7720

Fax: 1-309-762-9453

E-mail: [email protected]

www.parrinst.com

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