Parr-instrument Series 4558 Manual do Utilizador descarregar pdf (Página 3)

4555 - 58 Series

5G & 10L Pressure Reactors

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TABLE OF CONTENTS

TABLE OF CONTENTS............................ 2

Related Instructions........................... 3

Customer Service.............................. 3

PREFACE ................................................. 4

Scope ................................................ 4

Safety Information ............................. 4

Provisions for Lifting and Carrying..... 4

General Specifications....................... 5

Explanation of Symbols ..................... 6

Environmental Conditions.................. 6

Intended Usage ................................. 7

User’s Responsibility ......................... 7

Unpack Carefully ............................... 7

INSTALLATION ........................................ 8

Pressure, Temperature Limits ........... 8

Slave Box Control A1761HC3 ........... 8

ASSEMBLE THE REACTOR.................... 9

Removable Head Vessel ................... 9

Fixed Head Vessel .......................... 10

Cylinder Slide Adjustment................ 12

IDENTIFY THE VALVES......................... 13

Gas Inlet Valve ................................ 13

Gas Release Valve.......................... 13

Liquid Sampling Valve..................... 13

OTHER VESSEL HEAD FITTINGS ........ 14

Safety Rupture Disc......................... 14

Type J Thermocouple...................... 14

Pressure Gage ................................ 14

Gage and Valve Adapters................ 14

HOW TO USE THE VESSEL .................. 15

Flat Gasket or O-ring Seal............... 15

To Open the Vessel......................... 15

Before Closing the Vessel ............... 15

Close the Vessel.............................. 16

Gas Connections............................. 16

Pressurizing the Vessel ................... 16

Do Not Overfill ................................. 17

Releasing Pressure ......................... 17

Withdrawing Liquid Samples............17

The Shaft Seal .................................17

REACTORS WITH SLAVE BOX CONTROLS 18

3-Zone Slave Box A1761HCEE ........ 18

3-Zone Slave Box A1761HC3........... 18

Initial Operating Test......................... 18

ACCESSORIES........................................ 19

Internal Cooling Coils........................ 19

Stirrer Drive Systems........................ 19

Quick Disconnect Drive Coupler ....... 19

Air Motor ........................................... 20

Variable Speed Electric Motor .......... 20

Spare Parts Kit.................................. 20

EXPLOSION PROOF OPERATION......... 21

The Motor ......................................... 21

The Temperature Controller.............. 21

Slave Box Control ............................. 21

The Heater........................................ 21

The Wiring ........................................ 21

PERIODIC PRESSURE TESTS ............... 22

GENERAL MAINTENANCE NOTES........ 23

Fuses................................................ 24

PARTS LISTS........................................... 25

Vessel Parts List ............................... 25

Internal Fittings ................................. 25

External Fittings ................................ 26

Internal Parts Identification ............... 27

External Parts Identification .............. 28

Cooling Coils & Fittings..................... 29

Drive Parts List.................................. 30

Stands............................................... 31

Slave Boxes...................................... 31

Heaters ............................................. 32

APPENDIX A – REMOVABLE VESSEL

REACTOR DRAWINGS ........................... 33

APPENDIX B – FIXED HEAD VESSEL

REACTOR DRAWINGS ........................... 36

1 2 3 4 5 6 7 8 ... 47 48

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