Parr-instrument Series 5500 Manual do Utilizador descarregar pdf (Página 2)

Compact Micro Reactors

Parr Instrument Company

Preface 3

Scope 3

Related Instructions 3

Safety Information 3

General Speciﬁcations 3

Electrical Ratings 3

Explanation of Symbols 4

Environmental Conditions 4

Intended Usage 4

Provisions for Lifting and Carrying 4

Cleaning & Maintenance 4

User’s Responsibility 5

Unpack Carefully 5

Flat PTFE Gasket or Self Sealing O-Ring Closure 6

Installation 7

Pressure and Temperature Limits 7

Assemble The Reactor 8

Identify The Valves 9

Gas Inlet Valve 9

Gas Release Valve 9

Liquid Sampling Valve 9

Other Vessel Head Fittings 9

Safety Rupture Disc 9

Type J Thermocouple 9

Pressure Gage 9

How To Use The Vessel 10

Removable Head Vessel Flat Gasket Closure 10

To Open the Vessel 10

Before Closing the Vessel 10

To Close the Vessel 10

Sealing Vessels with PTFE Gaskets 10

O-Ring Closures 10

Gas Connections 10

Pressurizing the Vessel 10

Do Not Overﬁll the Vessel 11

Releasing Pressure 11

Withdrawing Liquid Samples 11

Initial Operating Test 11

Accessories 11

Liners 11

Spare Parts Kit 11

Periodic Pressure Tests 12

General Maintenance Notes 12

Parts Lists 13

Internal Fittings* 13

External Fittings* 13

Vessel Heaters Parts List 15

Drawings 16

Motor/Overarm Layout 16

Tach Option Layout 17

Parts included when apparatus is EMC compliant: 17

25 mL and 50 mL Vessel Assemblies 18

100 mL Vessel Assembly 19

Customer Service

Questions concerning the installation or operation

of this instrument can be answered by the Parr

Customer Service Department:

1-309-762-7716 • 1-800-872-7720

Fax: 1-309-762-9453

E-mail: [email protected]

http://www.parrinst.com

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