Parr-instrument 6200 Manual do Utilizador

Operating Instruction Manual No. 442M9 6200Oxygen Bomb Calorimeter

116200Calorimeter Operating Instruction ManualOverview The 6200 Calorimeter has been designed to provide the user with: • A traditional design ca

12 6200Calorimeter Operating Instruction ManualFull Micro-processor Based Process Control Full Micro-processor Based Data Acquisition and Handling

136200Calorimeter Operating Instruction ManualFilling the Jacket ReservoirPowerConnectionJacket Cooling Water Connection The 6200 Calorimeter is co

14 6200Calorimeter Operating Instruction ManualJacket Cooling Water Connection Continued Oxygen Filling Connection Printer and Balance Connections 2

156200Calorimeter Operating Instruction ManualRetightening Swagelok Tube Fittings When Swagelok Tube Fittings are used, the instructions for ins

16 6200Calorimeter Operating Instruction Manual Figure 2-1 6200 Calorimeter Back Panel 2-42

176200Calorimeter Operating Instruction Manual2 Line 1 & 2 – Maximum length of 10 feet -¼” OD, Polyurethane (Part Number HJ0025TB035) Line 3

18 6200Calorimeter Operating Instruction Manual Open Loop Configurations Figure 2-4 Figure 2-5 2-6 2

196200Calorimeter Operating Instruction ManualStandardizing the Calorimeter The calorimeter must be accurately standardized prior to actually perfo

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36200Calorimeter Operating Instruction ManualPreface I Scope...

216200Calorimeter Operating Instruction ManualControl Keys All calorimeter configurations and operations are handled by a menu-driven system operat

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236200Calorimeter Operating Instruction Manual The program in the 6200 Calorimeter can be extensively modified to tailor the unit to a wide variety

24 6200Calorimeter Operating Instruction ManualRevising Default Settings The default parameters of the 6200 Calorimeter can be changed to guarante

256200Calorimeter Operating Instruction ManualFigure 4- 1 6200 Factory Default Settings Calorimeter Operation Operating Mode Determination Bomb

26 6200Calorimeter Operating Instruction Manual4 Data Entry Controls Prompt for Bomb ID ON Weight Entry Mode Touch Screen Acid Entry Mode Touch

276200Calorimeter Operating Instruction ManualOperating the Filling Connection Detailed Instructions for preparing the sample and charging the 1108

28 6200Calorimeter Operating Instruction ManualOperating the Calorimeter All operations required to standardize the 6200 Calorimeter, or test an un

296200Calorimeter Operating Instruction Manual4. Set the bucket in the calorimeter. Attach the lifting handle (421A) to the two holes in the side

30 6200Calorimeter Operating Instruction Manual10. Remove all unburned pieces of fuse wire from the bomb electrodes; straighten them and measure the

4 6200Calorimeter Operating Instruction Manual Operating Instructions 5-1 Operating the 1108 Oxygen Bomb...

316200Calorimeter Operating Instruction Manual Particle Size and Moisture Content. Solid samples burn best in an oxygen bomb when reduced to 60 m

32 6200Calorimeter Operating Instruction ManualCombustion CapsulesCoarse Samples Non-volatile samples to be tested in Parr oxygen bombs are weighed

336200Calorimeter Operating Instruction ManualCorrosive Samples 5 The 1108 Oxygen Bomb is made of a corrosion resistant alloy designed to withstan

34 6200Calorimeter Operating Instruction Manual Use the following procedure when filling and handling any of these tape-sealed sample holders: •

356200Calorimeter Operating Instruction Manual Final reports for each test can be obtained whenever the operator is prepared to enter any required

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376200Calorimeter Operating Instruction ManualReportOption SelectionReport Generation The 6200 Calorimeter can transmit its stored test data in eit

38 6200Calorimeter Operating Instruction Manual The displayed files can be sorted by sample ID number, by type, by status or by date of test by sim

396200Calorimeter Operating Instruction ManualClearing Memory The 6200 Calorimeter will hold data for 1000 tests in its memory. These tests may be

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56200Calorimeter Operating Instruction ManualAppendix B – Calculations B-1 Calculating the Heat of Combustion...

416200Calorimeter Operating Instruction Manual Under normal usage the 1108 Parr Oxygen Bomb will give long service if handled with reasonable care.

42 6200Calorimeter Operating Instruction ManualThe replacement of protective fuses for the 6200 Calorimeter should be performed by qualified personn

436200Calorimeter Operating Instruction Manual A / D Initialization Failed. Shortly after power is applied to the calorimeter controller and the op

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456200Calorimeter Operating Instruction Manual The settings and controls are organized into nine main sections or pages which comprise the Main Men

46 6200Calorimeter Operating Instruction Manual Setup. Press this key to access the Temperature Plot Setup Menu, which has many keys tha

476200Calorimeter Operating Instruction Manual Time Units. Toggles between minutes and seconds. Bucket Plot Color. Toggles between: • Red • Green •

48 6200Calorimeter Operating Instruction ManualOperating Controls Menu Method of Operation. Offers an operating mode of either dynamic

496200Calorimeter Operating Instruction ManualProgram Information and Control Menu Calibrate Touchscreen. This key prompts the user to touch the sc

50 6200Calorimeter Operating Instruction ManualProgram Information and Control MenuContinuedCalibration Data and Controls Menu Save User Default Set

6 6200Calorimeter Operating Instruction Manual Figures 2-1 6200 Calorimeter Back Panel ...

516200Calorimeter Operating Instruction ManualCalibration and Data Controls Menu Continued EE Max Std Deviation. Displays the maximum relative stan

52 6200Calorimeter Operating Instruction ManualThermo-chemical Corrections MenuPrint Standardization Runs. Will print all of the tests that have bee

536200Calorimeter Operating Instruction ManualCalculation Factors. Accesses sub-menu, Calculation Factors which sets a number of options for the way

54 6200Calorimeter Operating Instruction ManualData Entry Controls Menu Prompt for Bomb ID. In the ON position the controller will pro

556200Calorimeter Operating Instruction ManualAuto Preweigh ID Controls. Accesses sub-menu, used to automatically assign Sample ID numbers when a se

56 6200Calorimeter Operating Instruction Manual Communication Controls. Accesses sub-menus which set the communications protocols for t

576200Calorimeter Operating Instruction ManualBalance Port (RS232). Accesses sub-menu, Balance Port Communications. Balance Type. This key toggl

58 6200Calorimeter Operating Instruction ManualFile Management MenuAPPENDIX A Run Data File Manager - This key activates the File Manager. The File

596200Calorimeter Operating Instruction ManualDiagnostics Menu APPENDIX A Allows the user to test many of the components and subsystems of the c

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76200Calorimeter Operating Instruction ManualScope This manual contains instructions for installing and operating the Parr 6200 Calorimeter. For ea

616200Calorimeter Operating Instruction ManualCalculating the Heat of CombustionGeneral Calculations The 6200 Calorimeter will automatically make a

62 6200Calorimeter Operating Instruction ManualThermochemical Corrections Nitric Acid Correction. In the high pressure oxygen environment within

636200Calorimeter Operating Instruction Manual Current ASTM, ISO, and British Standard Methods differ on their treatment of the nitric and sulfuric

64 6200Calorimeter Operating Instruction Manual• Total acid is the amount of base required to titrate the bomb washings (milliliters). • Nitric ac

656200Calorimeter Operating Instruction ManualAcid and Sulfur CorrectionsContinued Users may find it convenient to enter a fixed value for the acid

66 6200Calorimeter Operating Instruction Manual In the ASTM treatment, the correction for acid formation assumes that all the acid titrated is nitr

676200Calorimeter Operating Instruction Manualm Spiking SamplesConversion to Other Moisture BasesConversion to Net Heat of Combustion It is someti

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696200Calorimeter Operating Instruction ManualStandard Materials The Energy Equivalent Factor. The term “standardization”, as used here, denotes

70 6200Calorimeter Operating Instruction Manual The 6200 Calorimeter includes a provision for calculating and using a mean energy equivalent for ea

8 6200Calorimeter Operating Instruction ManualPREFACE Explanation of Symbols I On position O Off position ~ Alternating Current (AC) This CAUTION

716200Calorimeter Operating Instruction ManualPrinter Port Balance Port RS232C Connections The 6200 Calorimeter is also equipped with an RS232C port

72 6200Calorimeter Operating Instruction ManualSartoriousBalanceInterface Field Length polarity 1 space 1 data 8 space 1 stability 2 CR 1 LF 1 T

736200Calorimeter Operating Instruction ManualField Length data 9 CR 1 The data field should consist of 9 numeric characters (0 through 9, +, - a

74 6200Calorimeter Operating Instruction Manual Table D-2 6200 Calorimeter Run Data Template Field Desc

756200Calorimeter Operating Instruction Manual Calorimeter test data can be transferred to an Ethernet network connected computer using the FTP File

76 6200Calorimeter Operating Instruction Manual The following screenshot illustrates the contents of the calorimeter data directory as presented by

776200Calorimeter Operating Instruction Manual The calorimeter offers a web server service. Test reports can be viewed with a web browser using a UR

78 6200Calorimeter Operating Instruction Manual Clicking on the Sample Data tab displays a list of reports currently in the instrument memory.

796200Calorimeter Operating Instruction Manual Clicking on any given report will provide a display as follows.

80 6200Calorimeter Operating Instruction ManualBar Code PortNetwork Data Devices The use of barcodes in the laboratory has become a highly accurat

96200Calorimeter Operating Instruction ManualSafety Information To avoid electrical shock, always: 1. Use a properly grounded electrical outlet of

816200Calorimeter Operating Instruction Manual Should you need assistance in the operation or service of your instrument, please contact the Techni

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836200Calorimeter Operating Instruction Manual APPENDIX F 6200 CALORIMETER PARTS LIST Principal Asse

84 6200Calorimeter Operating Instruction ManualParts List for Temperature Control Assembly Item Description 1281DD 1417E 538VB 252HWHJ 280HWHJ A12

856200Calorimeter Operating Instruction ManualParts List for 6200 Stirrer Motor and Drive Item Description 1285DD 1241DD2 1242DD A1268DD Mount, Mot

86 6200Calorimeter Operating Instruction Manual Figure F-1 6200 Oxygen Bomb Calorimeter Cutaway Front F-4A

876200Calorimeter Operating Instruction Manual Figure F-2 6200 Oxygen Bomb Calorimeter Cutaway Rear F-5 A

88 6200Calorimeter Operating Instruction Manual F-6Figure F-3 A1279DD Control Schematic APPENDIX F

896200Calorimeter Operating Instruction Manual F-7 Figure F-4 Oxygen Solenoid Assembly & Fittings A

90 6200Calorimeter Operating Instruction Manual F-8Figure F-5 Water Tank Assembly APPENDIX F

10 6200Calorimeter Operating Instruction Manual These steps are offered to help the user become familiar with, install, operate and develop the full

916200Calorimeter Operating Instruction Manual F-9 Figure F-6 A1311DD Circulating Pump Assembly with Fittings APPENDIX F

92 6200Calorimeter Operating Instruction ManualF-10Figure F-7 Temperature Control Assembly with Fittings APPENDIX F

936200Calorimeter Operating Instruction ManualAPPENDIX F Figure F-8 A1284DD2 Stirrer Hub Assembly F-11

94 6200Calorimeter Operating Instruction Manual APPENDIX FF-12 Figure F-9 Stirrer Motor Assembly F-12

Revision 01/29/10 PARR INSTRUMENT COMPANY 211 Fifty - Third Street Moline, Illinois 61265 USA 309 / 762-7716 800 / 872-7720 Fax 309 / 7